Inorganic Chemistry (i)Gravimetric analysis : Barium as Barium sulphate, Copper as cuprous thiocynate. (ii)Complex compound preparation (a) Potassium chlorochromate (IV) (b) Tetramine copper (II) sulphate monohydrate (c) Hexamminenickel (II) chloride (iii)Effluent water analysis, Identification of cations and anions in different samples. (iv)Water analysis, To determine dissolved oxygen in water samples in ppm. Physical Chemistry (i)To determine the velocity constant (specific reaction rate) of hydrolysis of methyl acetate / ethyl acetate catalyzed by hydrogen ions at room temperature. (ii)Determination of partition coefficient of iodine between carbon tetrachloride and water. (iii)Job’s method. (iv)pH-metric titrations, conductometric titrations. Organic Chemistry 1.Binary mixture analysis containing two solids : Separation, Identification and Preparation of derivatives. 2.Preparation (i) Acetylation, (ii) Benzolylation, (iii) Meta dinitro benzene, (iv) Picric acid, P-Nitro Acetanilide, Dibenzylacetone Viva-voce Record
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